Soap-making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant

Εξώφυλλο
Van Nostrand, 1922 - 243 σελίδες

Αναζήτηση στο βιβλίο

Άλλες εκδόσεις - Προβολή όλων

Συχνά εμφανιζόμενοι όροι και φράσεις

Δημοφιλή αποσπάσματα

Σελίδα 226 - To find the velocity in feet per minute necessary to discharge a given volume of water in a given time, multiply the number of cubic feet of water by 144 and divide the product by the area of the pipe in inches.
Σελίδα 158 - ... developed locally by the alkali running into the mixture. When this point is reached the sides of the flask are washed down with carbon-dioxide-free water and the alkali subsequently added drop by drop, mixing after each drop until the desired tint is obtained.
Σελίδα 162 - Now add 50 cc. of 50 per cent. sulphuric acid (by volume) and immerse the vessel in boiling water for two hours and keep protected from dust and organic vapors, such as alcohol, till the titration is completed. Add from a weighing bottle a slight excess of the ferrous ammonium sulphate (C), making spot tests on a porcelain plate with the potassium ferricyanide (/.). Titrate back with the dilute bichromate. From the amount of bichromate reduced calculate the percentage of glycerol.
Σελίδα 158 - N/l acid (E) until the pinkish yellow or chosen end-point color just remains.* A further addition of the indicator at this point will cause an increase of the pink color; this must be neglected, and the first end-point taken.
Σελίδα 154 - The dish is then allowed to remain on a water bath or top of the oven until the excess water has evaporated and the residue is in such a condition that on returning to the oven at 160° C. it will not spit. The time taken up to this point cannot be given definitely, nor is it important. Usually two to three hours is required.
Σελίδα 159 - The result will include acetylisable impurities, if any be present. 2. Determine the total residue at 160° C. 3. Determine the acetin value of the residue at (2) in terms of glycerol. 4. Deduct the result found at (3) from the percentage obtained at (1) and report this corrected figure as glycerol. If volatile acetylisable impurities are present, these are included in this figure.
Σελίδα 220 - System The fundamental unit of the metric system is the Meter — the unit of length. From this the units of capacity (Liter) and of weight (Gram) were derived. All other units are the decimal subdivisions or multiples of these. These three units are simply related; eg. for all practical purposes one Cubic Decimeter equals one Liter and one Liter of water weighs one Kilogram.
Σελίδα 153 - ... or most of it, should be evaporated off at this temperature. When only a slight vapour is seen to come off, the dish is removed and allowed to cool. An addition of...
Σελίδα 156 - ... results may be incorrect. Into a stoppered weighing bottle containing a known weight of recently distilled aniline (from 10 to 20 cc.) measure about 2 cc. of the sample, stopper, mix, cool, and weigh. Wash the contents into about 200 cc. of cold water, and titrate the acidity as before. This yields the acidity due to the original preformed acetic acid, plus...
Σελίδα 157 - The object of cooling is to avoid any sudden rush of vapors from the flask on adding water, and to avoid breaking the flask. Time is saved by adding the water before the contents of the flask solidify, but the contents may be allowed to solidify and the test proceeded with the next day without detriment, bearing in mind that the anhydride in excess is much more effectively hydrolyzed in hot than in cold water.

Πληροφορίες βιβλιογραφίας